EN 71-3 2012 [复制链接]

也不知道新的EN 71-3 标准到底进行到什么程度了，翻遍了网络，只找到了最新的Draft的目录，大家将就看看吧（能看到新版的草案中已经给出了有机锡和铬形态分析的具体方法，包括具体要测试的有机锡的种类，等等）。十分期待有人放出全文！ ,tTq25~H\  
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Foreword "%I<yUP]U  
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Introduction 'vwu^u?  
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1 Scope b^:frjaE3  
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2 Normative references A('o&H  
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3 Terms and definitions icK$W2<8mg  
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4 Requirements j=dGNi)R  
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4.1 Categories of toy materials T' =6_?7K4  
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4.1.1 Category I: Dry, brittle, dust-like or pliable material ~ <36vsk  
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4.1.2 Category II: Liquid or adhesive material ~8&P*oFC  
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4.1.3 Category III: material scraped Kzx` E>,z'  
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4.1.4 Categories of different toy materials 2>[xe  
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4.2 Specific Requirements Bg[_MDWc-P  
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5 Short Description ]N2! 'c  
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6 Reagents and Equipment JEs@ky?{z  
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1.6 Reagents xI_0`@do  
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6.2 Device {+]tx4 6$  
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7 Sampling and Sample Preparation Gr>CdB>~+  
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7.1 Selection of samples for analysis .SLpgYFL{  
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7.2 Preparation of standards -&Q+x,.%  
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7.3 Sample Preparation O c.fvP^ZD  
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7.3.1 Category I: Dry, brittle, smooth or powdery materials and Category II: Liquid or sticky materials /O
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7.3.2 Category III: material scraped t\h4-dJn  
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4.7 migration procedures w3 kkam"  
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7.4.1 General &CcW(-  
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7.4.2 Category I: Dry, brittle, smooth or powdery materials and Category II: Liquid or sticky materials Faa>bc~E  
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7.4.3 Category III: material scraped LR{bNV[i  
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8 Analysis Method ]jY^*o[  
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8.1 General d:w/{m%#  
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8.2 Chromium (VI) (speciation) Jfk
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3.8 Organotin 39hep8+  
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9 Calculation of results %#rtNDi  
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9.1 Standard Elements FZn1$_Svr  
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9.1.1 Calibration Curves Z$g'h1,zW  
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9.1.2 Calculation of the concentration br Iz8]  
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9.1.3 Evaluation #O! 2
 
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9.2 Chromium (III) and chromium (VI) 2I}+AW!!=  
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9.2.1 Calibration Curves T0")Ryu  
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9.2.2 Calculation of the concentration F<4:P=  
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9.2.3 Evaluation  y705  
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3.9 Organotin \fEG 5/s}T  
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9.3.1 Calibration Curves &_-=(rK  
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9.3.2 Calculation of the migration of individual organotin compounds T@.+bD  
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9.3.3 Calculation of the migration of organotin ;Us6:}s  
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9.3.4 Evaluation ;"Qq/knVL  
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10 Test report ]}].Aq  
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Annex A (informative) Significant technical changes between this European Standard and the previous version 75^*4[  
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Annex B (informative) Results of laboratory proficiency testing - migration of elements (May 2012) flqr["czwK  
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Annex C (normative) Requirements for Sieve <:/aiX8  
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Annex D (informative) Preparation and analysis of the sample ~h8k4eM  
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Annex E (informative) Preparation of standards 7mi*#X}  
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E.1 ICP-MS W 3\+51P  
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E.1.1 stock solution (M1) ~!TrC<ft  
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E.1.2 Diluted stock solution (M2) ^8oN~HLZ  
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E.1.3 Work Solutions md{1Jn"  
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E.2 ICP-OES C|FI4/-e  
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E.2.1 stock solution (M1) olo9YrHn  
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E.2.2 Work Solutions 8_D:#i  
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Annex F (informative) Analysis Method cru&nH*O^  
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F.1 ICP-parameter Pvkr$ou  
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F.2 method for speciation of chromium G7-.d/8|^  
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F.2.1 Scope >
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F.2.2 Summary LGRhCOP:  
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F.2.3 reagents Y5IQhV.  
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F.2.4 test equipment F*B^#AZg  
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F.2.5 Method 8`b_,(\N  
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F.2.6 reporting NydoX9  
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F.2.7 Example for LC-ICP-MS conditions kvt"7;(  
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F.3 procedures for organotin r<kqs,-~  
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F.3.1 Scope pe`&zI_`?  
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F.3.2 terms /{X2:g{  
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F.3.3 Summary qc^qCGy!z  
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F.3.4 reagents z 4`H<Pn  
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F.3.5 test equipment _"";SqVB  
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F.3.6 process -u'BK@;
  
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F.3.7 Example for the gas chromatography conditions L[:b\O/p,  
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Annex G (informative) Rationale &!FWo@  
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G.1 skin contact (scope) KF`@o@,  
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G.2 organotin (F.3.7.2) 09u@
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Annex H (informative) Additional information on inspection of certain elements [P23.`G~J  
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Annex ZA (informative) Relationship between this European Standard and the Essential Requirements of EU Directive 2009/48/EC (If (created in due time)) aC2\C=ru_  
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References CwVORf,uA