EN 71-3 2012 [复制链接]

也不知道新的EN 71-3 标准到底进行到什么程度了，翻遍了网络，只找到了最新的Draft的目录，大家将就看看吧（能看到新版的草案中已经给出了有机锡和铬形态分析的具体方法，包括具体要测试的有机锡的种类，等等）。十分期待有人放出全文！ -MBxl`JU  
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Foreword VuZr:-K/  
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Introduction E ' uZA  
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1 Scope [dVL&k<P  

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2 Normative references F_P~x(X  
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3 Terms and definitions <%mRSv  
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4 Requirements 0b 54fD=  
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4.1 Categories of toy materials r: :b  
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4.1.1 Category I: Dry, brittle, dust-like or pliable material UC$ppTCc?  
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4.1.2 Category II: Liquid or adhesive material Zb#u0Tq  
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4.1.3 Category III: material scraped .A|@?p[  
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4.1.4 Categories of different toy materials R^e'}+Z  
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4.2 Specific Requirements UL9n-M=  
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5 Short Description L4 l!96]a  
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6 Reagents and Equipment %xt^698&X  
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1.6 Reagents Ht YwEjI  
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6.2 Device ??/ 'kmd  
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7 Sampling and Sample Preparation BfiD9ka-z  
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7.1 Selection of samples for analysis XRQ4\bMA8  
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7.2 Preparation of standards | VDV<g5h  
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7.3 Sample Preparation "5$B>S(Q  
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7.3.1 Category I: Dry, brittle, smooth or powdery materials and Category II: Liquid or sticky materials 18:%~ >.!  
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7.3.2 Category III: material scraped %ULr8)R;  
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4.7 migration procedures >b4eL59  
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7.4.1 General \dQNLLg/  
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7.4.2 Category I: Dry, brittle, smooth or powdery materials and Category II: Liquid or sticky materials wLr_-vJ  
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7.4.3 Category III: material scraped <2qr}K{'A  
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8 Analysis Method ]OzUGXxo~  
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8.1 General d6 5L!4  
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8.2 Chromium (VI) (speciation) 92KRb;c  
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3.8 Organotin ~Jz6O U*z  
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9 Calculation of results :20W\P<O!A  
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9.1 Standard Elements oM
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9.1.1 Calibration Curves yO~Ig `w  
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9.1.2 Calculation of the concentration Y`SvMkP)+  
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9.1.3 Evaluation 0.k7oB;f(@  
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9.2 Chromium (III) and chromium (VI) v #j$;  
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9.2.1 Calibration Curves y/ ef>ZZ  
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9.2.2 Calculation of the concentration 1NA.nw.  
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9.2.3 Evaluation CN8Y\<Ar  
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3.9 Organotin z/@slT  
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9.3.1 Calibration Curves &powy7rR  
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9.3.2 Calculation of the migration of individual organotin compounds DAr1 C+Dy  
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9.3.3 Calculation of the migration of organotin eiaF
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9.3.4 Evaluation =|y9UlsD  
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10 Test report T<Z &kYU:R  
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Annex A (informative) Significant technical changes between this European Standard and the previous version RmeD$>7  
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Annex B (informative) Results of laboratory proficiency testing - migration of elements (May 2012) u5b|#&-mX  
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Annex C (normative) Requirements for Sieve rCbDu&k]  
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Annex D (informative) Preparation and analysis of the sample G+"t/?/  
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Annex E (informative) Preparation of standards *-=(Q`3  
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E.1 ICP-MS FQ7T'G![  
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E.1.1 stock solution (M1) 2Aazy'/  
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E.1.2 Diluted stock solution (M2) +_?hK{Ib"  
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E.1.3 Work Solutions Yz/md1T$  
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E.2 ICP-OES 6ryak!|[  
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E.2.1 stock solution (M1) &Fzb6/  
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E.2.2 Work Solutions MSQEO4ge  
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Annex F (informative) Analysis Method w(*vj  
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F.1 ICP-parameter axv>6k  
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F.2 method for speciation of chromium ?>D+ge  
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F.2.1 Scope Gv!2f  
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F.2.2 Summary ajbA\/\G;  
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F.2.3 reagents :KSV4>X[%a  
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F.2.4 test equipment VZp5)-!\  
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F.2.5 Method
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F.2.6 reporting "(3[+W{|  
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F.2.7 Example for LC-ICP-MS conditions A9KET$i@v  
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F.3 procedures for organotin b<tNk]7  
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F.3.1 Scope f$o_e90mu  
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F.3.2 terms ")1:F>  
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F.3.3 Summary 'NbHa!  
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F.3.4 reagents ~V:\ _{mE  
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F.3.5 test equipment "-Mp_O]  
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F.3.6 process j\ZXG=j  
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F.3.7 Example for the gas chromatography conditions I <DL=V  
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Annex G (informative) Rationale E[O J+ ;c  
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G.1 skin contact (scope) SA:Zc^a V  
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G.2 organotin (F.3.7.2) mb1FWy=3  
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Annex H (informative) Additional information on inspection of certain elements 7K12 G!)  
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Annex ZA (informative) Relationship between this European Standard and the Essential Requirements of EU Directive 2009/48/EC (If (created in due time)) I
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References H;mSkRD3N