也不知道新的EN 71-3 标准到底进行到什么程度了,翻遍了网络,只找到了最新的Draft的目录,大家将就看看吧(能看到新版的草案中已经给出了有机锡和铬形态分析的具体方法,包括具体要测试的有机锡的种类,等等)。十分期待有人放出全文! YBR)s\*
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Foreword zkH<aLRB
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Introduction R,uJK)m
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1 Scope ='KPT1dW*
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2 Normative references Lqg7D\7j
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3 Terms and definitions GcPB'`!M
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4 Requirements R/yPZO-U
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4.1 Categories of toy materials M|5^
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4.1.1 Category I: Dry, brittle, dust-like or pliable material I #Arr#%
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4.1.2 Category II: Liquid or adhesive material %w;1*~bH
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4.1.3 Category III: material scraped rjq -ZrC%
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4.1.4 Categories of different toy materials qg/Y;tGSx
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4.2 Specific Requirements QSlf=VK*y
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5 Short Description mE)x7
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6 Reagents and Equipment C={sE*&dYX
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1.6 Reagents FuRn%)DA5
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6.2 Device ^;v.ytO*
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7 Sampling and Sample Preparation :{e`$kz
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7.1 Selection of samples for analysis yDl5t-0`
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7.2 Preparation of standards HvL9;^!
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7.3 Sample Preparation @5POgQ8
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7.3.1 Category I: Dry, brittle, smooth or powdery materials and Category II: Liquid or sticky materials a-o
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7.3.2 Category III: material scraped h_}BmJ h_
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4.7 migration procedures 9fk\Ay1P
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7.4.1 General ?PH}b?f4
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7.4.2 Category I: Dry, brittle, smooth or powdery materials and Category II: Liquid or sticky materials D6@4
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7.4.3 Category III: material scraped J0Rz.=Y
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8 Analysis Method =.3P)gY)
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8.1 General _S7M5{U_
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8.2 Chromium (VI) (speciation) w[n>4?"{
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3.8 Organotin &?ed.V@E5
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9 Calculation of results 26klW:2*
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9.1 Standard Elements 8f`b=r(a>
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9.1.1 Calibration Curves ?;=Y1O7N(
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9.1.2 Calculation of the concentration .}u(&
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9.1.3 Evaluation !-}*jm p<
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9.2 Chromium (III) and chromium (VI) }(7QJk5 j
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9.2.1 Calibration Curves ,f""|X5
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9.2.2 Calculation of the concentration
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9.2.3 Evaluation a/`Yh>ou
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3.9 Organotin m6ws#%|[
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9.3.1 Calibration Curves %Yn)t3d
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9.3.2 Calculation of the migration of individual organotin compounds JBJ7k
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9.3.3 Calculation of the migration of organotin s7.*o@G
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9.3.4 Evaluation ZvKMRW
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10 Test report 6(^9D_"@
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Annex A (informative) Significant technical changes between this European Standard and the previous version ?a9k5@s
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Annex B (informative) Results of laboratory proficiency testing - migration of elements (May 2012) fb;"J+
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Annex C (normative) Requirements for Sieve j7+t@DqQ
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Annex D (informative) Preparation and analysis of the sample i)3\jO0&GU
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Annex E (informative) Preparation of standards kweTK]mT
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E.1 ICP-MS %"^XxVJ*
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E.1.1 stock solution (M1) [wG%@0\
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E.1.2 Diluted stock solution (M2) N+75wtLy&
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E.1.3 Work Solutions c10).zZ
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E.2 ICP-OES `0D1Nh"%k
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E.2.2 Work Solutions 6Qu*'
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Annex F (informative) Analysis Method j56 An6g
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F.1 ICP-parameter X+8p2xSO|
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F.2 method for speciation of chromium
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F.2.1 Scope c"1d#8J
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F.2.2 Summary 1+($"$ZC&B
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F.2.3 reagents +~O{
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F.2.4 test equipment 9YhsJ~"Q
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F.2.5 Method 'qE
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F.2.6 reporting [rU8
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F.2.7 Example for LC-ICP-MS conditions GJPZ[bo
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F.3 procedures for organotin |>GIPfVT
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F.3.1 Scope _Qc\v0%
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F.3.3 Summary ,5*xE\9G
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F.3.4 reagents REBDr;tv
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F.3.6 process 5>Yd\(`K
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F.3.7 Example for the gas chromatography conditions ld:alEo
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Annex G (informative) Rationale ^T6!z^g1h
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G.1 skin contact (scope) Go7hDmu
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G.2 organotin (F.3.7.2) 4,ynt&
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Annex H (informative) Additional information on inspection of certain elements $=xQ X
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Annex ZA (informative) Relationship between this European Standard and the Essential Requirements of EU Directive 2009/48/EC (If (created in due time)) f,inQ2f}d
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References bRz^=