也不知道新的EN 71-3 标准到底进行到什么程度了,翻遍了网络,只找到了最新的Draft的目录,大家将就看看吧(能看到新版的草案中已经给出了有机锡和铬形态分析的具体方法,包括具体要测试的有机锡的种类,等等)。十分期待有人放出全文! nbP}a?XC
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Foreword U&B(uk(2
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Introduction / zNVJhC
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1 Scope \)\n5F:Zu
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2 Normative references AX@bM
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3 Terms and definitions >/C,1}p[
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4 Requirements DP*V|
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4.1 Categories of toy materials }/NL"0j+4
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4.1.1 Category I: Dry, brittle, dust-like or pliable material )J\
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4.1.2 Category II: Liquid or adhesive material ~ebm,3?
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4.1.3 Category III: material scraped ir)~T0
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4.1.4 Categories of different toy materials <e8
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4.2 Specific Requirements h5H#xoCXp
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5 Short Description ?B4X&xf.D
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6 Reagents and Equipment %LdFS~
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1.6 Reagents -+|{#cz
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6.2 Device Rwz (20n\^
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7 Sampling and Sample Preparation v4x1=E
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7.1 Selection of samples for analysis SA16Ng
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7.2 Preparation of standards FY;R
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7.3 Sample Preparation :s OsG&y
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7.3.1 Category I: Dry, brittle, smooth or powdery materials and Category II: Liquid or sticky materials U#!f^@&AB
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7.3.2 Category III: material scraped 9Iod[ x
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4.7 migration procedures .-g++f(_i
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7.4.1 General ;:l\_b'Z}
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7.4.2 Category I: Dry, brittle, smooth or powdery materials and Category II: Liquid or sticky materials t:G67^<3
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7.4.3 Category III: material scraped .;0?r9
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8 Analysis Method X;I;CZ={
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8.1 General H)),
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8.2 Chromium (VI) (speciation) !?o661+b
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3.8 Organotin $\|$ekil4
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9 Calculation of results U}55;4^LX
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9.1 Standard Elements }vRs n-E@
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9.1.1 Calibration Curves 2t3'"8xJ
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9.1.2 Calculation of the concentration xF'9`y^]!@
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9.1.3 Evaluation ~VZ)LQ'7
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9.2 Chromium (III) and chromium (VI) YN1P9j#0d
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9.2.1 Calibration Curves fRp+-QvE
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9.2.2 Calculation of the concentration e_Na_l]
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9.2.3 Evaluation RF/I*5
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3.9 Organotin Fp>iwdjFg
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9.3.1 Calibration Curves 3+mC96wN
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9.3.2 Calculation of the migration of individual organotin compounds 5z8CUDt
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9.3.3 Calculation of the migration of organotin 5)fEs.r0
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9.3.4 Evaluation /QDlm>FM4
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Annex A (informative) Significant technical changes between this European Standard and the previous version t]?u<KD<
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Annex B (informative) Results of laboratory proficiency testing - migration of elements (May 2012) .a._WZF
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Annex C (normative) Requirements for Sieve q{/>hvl
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Annex D (informative) Preparation and analysis of the sample t}LV[bj1u
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Annex E (informative) Preparation of standards ]j
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E.1.2 Diluted stock solution (M2) YCvIB'
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E.2 ICP-OES 5U)Ia>p
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Annex F (informative) Analysis Method ]PWK^-4P
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F.2 method for speciation of chromium fTb&k;'LR<
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F.2.1 Scope WdQR^'b$
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F.2.2 Summary &y\7pAT\
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F.2.5 Method iX]tL:,~i
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F.2.6 reporting WdtZ{H
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F.2.7 Example for LC-ICP-MS conditions luvxwved
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F.3 procedures for organotin NuEcTww
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F.3.1 Scope UlNx5l+k
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F.3.3 Summary (F+]h]KSi
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F.3.5 test equipment Hfo/\\
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F.3.6 process [M#I Nm}
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F.3.7 Example for the gas chromatography conditions GhC%32F
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Annex G (informative) Rationale V8947h|&
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G.1 skin contact (scope) 7J|eL
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G.2 organotin (F.3.7.2) !{S HlS
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Annex H (informative) Additional information on inspection of certain elements P~@.(hed
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Annex ZA (informative) Relationship between this European Standard and the Essential Requirements of EU Directive 2009/48/EC (If (created in due time)) ~PA6e+gmL
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References m<GJ1)%3i